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Optimization of methyl orange removal from aqueous solution by response surface methodology using spenttea leaves as adsorbent

Liangzhi LI,Xiaolin LI,Ci YAN,Weiqiang GUO,Tianyi YANG,Jiaolong FU,Jiaoyan TANG,Cuiying HU

《环境科学与工程前沿（英文）》 2014年 第8卷 第4期   页码 496-502 doi: 10.1007/s11783-013-0578-0

摘要： The effective disposal of redundant tea waste is crucial to environmental protection and comprehensive utilization of trash resources. In this work, the removal of methyl orange (MO) from aqueous solution using spent tea leaves as the sorbent was investigated in a batch experiment. First, the effects of various parameters such as temperature, adsorption time, dose of spent tea leaves, and initial concentration of MO were investigated. Then, the response surface methodology (RSM), based on Box–Behnken design, was employed to obtain the optimum adsorption conditions. The optimal conditions could be obtained at an initial concentration of MO of 9.75 mg·L , temperature of 35.3°C, contact time of 63.8 min, and an adsorbent dosage 3.90 g·L . Under the optimized conditions, the maximal removal of MO was 58.2%. The results indicate that spent tea leaves could be used as an effective and economical adsorbent in the removal of MO from aqueous solution.

关键词： spent tea leaves     adsorption     response surface methodology     methyl orange (MO)    

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Separation of epigallocatechin-3-gallate from crude tea polyphenols by using Cellulose diacetate graft

Hong ZHU, Peiyong QIN

《化学科学与工程前沿（英文）》 2011年 第5卷 第3期   页码 330-338 doi: 10.1007/s11705-010-1104-6

摘要： This study demonstrates a new Cellulose diacetate graft -cyclodextrin (CDA- -CD) copolymer asymmetric membrane prepared by a phase inversion technique for the separation of (-)-epigallocatechin-3-gallate (EGCG) from other polyphenols in crude tea. The graft copolymer, CDA- -CD, was synthesized by prepolymerization of cellulose diacetate (CDA) and 1,6-hexamethylene-diisocyanate (HDI), which was then grafted with -cyclodextrin ( -CD). Surface and cross-section morphologies of the CDA- -CD membranes were analyzed by using scanning electron microscopy (SEM). Fourier transform infrared spectroscopy (FT-IR) indicated that the -CD was grafted onto the CDA by chemical bonding. The influences of the HDI/CDA mass ratio and the catalyst mass fraction on the -CD graft yield were investigated. The optimum conditions of a HDI/CDA mass ratio of 0.35 g·g and a catalyst mass fraction of 0.18 wt-% produced a -CD graft yield of 26.51 wt-%. The effects of the -CD graft yield and the concentration of the polymer cast solution on the separation of EGCG were also investigated. Under optimum conditions of a -CD graft yield of 24.21 wt-% and a polymer concentration of 13 wt-%, the purity of EGCG increased from 26.51 to 86.91 wt-%.

关键词： (-)-epigallocatechin-3-gallate (EGCG)     tea polyphenols     CDA-β-CD    

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Investigation of phosphate adsorption from an aqueous solution using spent fluid catalytic cracking catalyst

Zhen Li, Zhaofu Qiu, Ji Yang, Benteng Ma, Shuguang Lu, Chuanhui Qin

《环境科学与工程前沿（英文）》 2018年 第12卷 第6期 doi: 10.1007/s11783-018-1082-3

摘要：

Spent FCC catalyst with lanthanum is proposed as a novel P-removal adsorbent.

The spent FCC catalyst exhibits 99% adsorption efficiency for low P-concentration wastewater (C0 <5.0 mg/L).

High affinity, endothermic reaction and fast sorption kinetics are achieved.

The phosphate is adsorbed in the form of LaPO4 and KH2PO4.

关键词： Spent FCC catalyst     Phosphate removal     Adsorption     Lanthanum    

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APPLICATION AND DEVELOPMENT OF ‘GREEN’ PREVENTIVE AND CONTROL TECHNOLOGIES IN GUIZHOU TEA PLANTATIONS

《农业科学与工程前沿（英文）》 2022年 第9卷 第1期   页码 75-81 doi: 10.15302/J-FASE-2021424

摘要：

● Application of plant defense inducers against tea diseases.

关键词： ‘green’ prevention     natural enemies     plant defense inducers     tea plantations     Trifolium repens    

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INTERCROPPING TEA PLANTATIONS WITH SOYBEAN AND RAPESEED ENHANCES NITROGEN FIXATION THROUGH SHIFTS IN

《农业科学与工程前沿（英文）》 2022年 第9卷 第3期   页码 344-355 doi: 10.15302/J-FASE-2022451

摘要：

● Intercropping change soil bacterial communities in tea plantations.

关键词： intercropping     rapeseed     soil microbe     soybean     tea garden    

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APPLICATION AND DEVELOPMENT OF ‘GREEN’ PREVENTIVE AND CONTROL TECHNOLOGIES IN GUIZHOU TEA PLANTATIONS

《农业科学与工程前沿（英文）》 2022年 第9卷 第1期 doi: 0.15302/J-FASE-2021424

摘要：

The application and development of ‘green’ preventive technologies in tea plantations is an important means of ensuring tea quality and ecological safety. Ecological, agronomic and biological controls are the main preventive measures used in Guizhou Province. This paper summarizes the ‘green’ preventive technologies being applied in Guizhou tea plantations, including the use of plant defense inducers to regulate tea plant responses to pathogens, natural enemies to control pest species causing damage to shoots and Trifolium repens to control the main weed species. In addition, it summarizes the integrated ‘green’ preventive technologies being used in Guizhou and provides a foundation for the ecological maintenance of tea plantations. 

 

关键词： ‘green’ prevention / natural enemies / plant defense inducers / tea plantations / Trifolium repens    

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GASEOUS REACTIVE NITROGEN LOSSES FROM ORCHARDS, VEGETABLES AND TEA PLANTATIONS

《农业科学与工程前沿（英文）》 2023年 第10卷 第2期   页码 155-166 doi: 10.15302/J-FASE-2022477

摘要：

● Gaseous N emissions from orchards, vegetables and tea plantations (OVT) are reviewed.

关键词： fruit     greenhouse gas     green development     fertilizer management     climate change    

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Preparing graphene from anode graphite of spent lithium-ion batteries

Wenxuan Zhang, Zhanpeng Liu, Jing Xia, Feng Li, Wenzhi He, Guangming Li, Juwen Huang

《环境科学与工程前沿（英文）》 2017年 第11卷 第5期 doi: 10.1007/s11783-017-0993-8

摘要： With extensive use of lithium ion batteries (LIBs), amounts of LIBs were discarded, giving rise to growth of resources demand and environmental risk. In view of wide usage of natural graphite and the high content (12%–21%) of anode graphite in spent LIBs, recycling anode graphite from spent LIBs cannot only alleviate the shortage of natural graphite, but also promote the sustainable development of related industries. After calcined at 600°Cfor 1 h to remove organic substances, anode graphite was used to prepare graphene by oxidation-reduction method. Effect of pH and N2H4·H2O amount on reduction of graphite oxide were probed. Structure of graphite, graphite oxide and graphene were characterized by XRD, Raman and FTIR. Graphite oxide could be completely reduced to graphene at pH 11 and 0.25 mL N2H4·H2O. Due to the presence of some oxygen-containing groups and structure defects in anode graphite, concentrated H2SO4 and KMnO4 consumptions were 40% and around 28.6% less than graphene preparation from natural graphite, respectively.

关键词： Spent LIBs     Graphite     Graphite oxide     Grapheme    

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TRANSCRIPTOME ANALYSIS REVEALS METABOLITE VARIATION AND FLAVONOID REGULATORY NETWORKS IN FRESH SHOOTS OF TEA

《农业科学与工程前沿（英文）》 2021年 第8卷 第2期

摘要：

Metabolites, especially secondary metabolites, are very important in the adaption of tea plants and the quality of tea products. Here, we focus on the seasonal variation in metabolites of fresh tea shoots and their regulatory mechanism at the transcriptional level. The metabolic profiles of fresh tea shoots of 10 tea accessions collected in spring, summer, and autumn were analyzed using ultra-performance liquid chromatography coupled with quadrupole-obitrap mass spectrometry. We focused on the metabolites and key genes in the phenylpropanoid/flavonoid pathway integrated with transcriptome analysis. Multivariate statistical analysis indicates that metabolites were distinctly different with seasonal alternation. Flavonoids, amino acids, organic acids and alkaloids were the predominant metabolites. Levels of most key genes and downstream compounds in the flavonoid pathway were lowest in spring but the catechin quality index was highest in spring. The regulatory pathway was explored by constructing a metabolite correlation network and a weighted gene co-expression network.

 

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TRANSCRIPTOME ANALYSIS REVEALS METABOLITE VARIATION AND FLAVONOID REGULATORY NETWORKS IN FRESH SHOOTS OF TEA

Chen-Kai JIANG, De-Jiang NI, Ming-Zhe YAO, Jian-Qiang MA, Liang CHEN

《农业科学与工程前沿（英文）》   页码 215-230 doi: 10.15302/J-FASE-2021382

摘要： Metabolites, especially secondary metabolites, are very important in the adaption of tea plants and the quality of tea products. Here, we focus on the seasonal variation in metabolites of fresh tea shoots and their regulatory mechanism at the transcriptional level. The metabolic profiles of fresh tea shoots of 10 tea accessions collected in spring, summer, and autumn were analyzed using ultra-performance liquid chromatography coupled with quadrupole-obitrap mass spectrometry. We focused on the metabolites and key genes in the phenylpropanoid/flavonoid pathway integrated with transcriptome analysis. Multivariate statistical analysis indicates that metabolites were distinctly different with seasonal alternation. Flavonoids, amino acids, organic acids and alkaloids were the predominant metabolites. Levels of most key genes and downstream compounds in the flavonoid pathway were lowest in spring but the catechin quality index was highest in spring. The regulatory pathway was explored by constructing a metabolite correlation network and a weighted gene co-expression network.

关键词： harvest season     metabolites     tea shoots     transcriptomics     untargeted metabolomics    

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Highly selective metal recovery from spent lithium-ion batteries through stoichiometric hydrogen ion

Weiguang Lv, Xiaohong Zheng, Li Li, Hongbin Cao, Yi Zhang, Renjie Chen, Hancheng Ou, Fei Kang, Zhi Sun

《化学科学与工程前沿（英文）》 2021年 第15卷 第5期   页码 1243-1256 doi: 10.1007/s11705-020-2029-3

摘要： Spent lithium-ion battery recycling has attracted significant attention because of its importance in regard to the environment and resource importance. Traditional hydrometallurgical methods usually leach all valuable metals and subsequently extract target meals to prepare corresponding materials. However, Li recovery in these processes requires lengthy operational procedures, and the recovery efficiency is low. In this research, we demonstrate a method to selectively recover lithium before the leaching of other elements by introducing a hydrothermal treatment. Approximately 90% of Li is leached from high-Ni layered oxide cathode powders, while consuming a nearly stoichiometric amount of hydrogen ions. With this selective recovery of Li, the transition metals remain as solid residue hydroxides or oxides. Furthermore, the extraction of Li is found to be highly dependent on the content of transition metals in the cathode materials. A high leaching selectivity of Li (>98%) and nearly 95% leaching efficiency of Li can be reached with LiNi Co Mn O . In this case, both the energy and material consumption during the proposed Li recovery is significantly decreased compared to traditional methods; furthermore, the proposed method makes full use of H to leach Li . This research is expected to provide new understanding for selectively recovering metal from secondary resources.

关键词： recycling     spent LIBs     selective recovery     hydrothermal treatment    

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Bioleaching of spent Ni-Cd batteries and phylogenetic analysis of an acidophilic strain in acidified

ZHAO Ling, WANG Liang, YANG Dong, ZHU Nanwen

《环境科学与工程前沿（英文）》 2007年 第1卷 第4期   页码 459-465 doi: 10.1007/s11783-007-0073-6

摘要： Biohydrometallurgy is a novel method to recycle discarded batteries, in which sewage sludge is used as microorganisms and culture due to the presence of indigenous . A two-step continuous flow leaching system co

关键词： Biohydrometallurgy     discarded     indigenous     two-step continuous     presence    

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Alcohol and tea consumption in relation to the risk of nasopharyngeal carcinoma in Guangdong, China

Hong-Lian RUAN, Feng-Hua XU, Wen-Sheng LIU, Qi-Sheng FENG, Li-Zhen CHEN, Yi-Xin ZENG, Wei-Hua JIA,

《医学前沿（英文）》 2010年 第4卷 第4期   页码 448-456 doi: 10.1007/s11684-010-0280-6

摘要： To investigate whether alcohol and tea consumption has an etiological association with nasopharyngeal carcinoma (NPC) in a high-incident population, a large scale case-control study was conducted. The study included 2846 individuals in Guangdong Province, China, with 1387 newly diagnosed cases of NPC and 1459 frequency-matched controls. Exposure histories of alcohol and tea consumption were obtained via personal interviews. Information regarding socio-demographic characteristics (age, sex, education, dialect and household type), family history of NPC, Epstein-Barr virus (EBV) infection, dietary habits and other potential confounding factors was also studied. An analysis was performed using unconditional logistic regression to calculate odds ratios (OR) and 95% confidence intervals (CI). The risk of NPC was found to be associated with habitual alcohol consumption and tea consumption. Tea consumption has been associated with a decreased occurrence of NPC (OR= 0.62), while consumption of alcohol was associated with a complex effect. Specifically, moderate consumption of alcohol was associated with decreased risk of NPC, while overuse, especially strong distillate spirits, appeared to be a risk factor.

关键词： nasopharyngeal carcinoma     case-control study     alcohol consumption     tea consumption    

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A comparison of the biological activities of ethyl acetate fractions from the stems and leaves of

Zhaolei WANG, Kai JIANG, Qinchao DING, Shujun LIU, Xiaobing DOU, Bin DING

《农业科学与工程前沿（英文）》 2020年 第7卷 第4期   页码 505-512 doi: 10.15302/J-FASE-2019271

摘要：

Pursh (PCP) is a popular traditional medicinal plant in China, widely used for the treatment of a variety of liver diseases. Although it has been long recognized that the main active elements of PCP are contained in ethyl acetate fraction (EAF), little is known so far in terms of the relative effectiveness of EAF derived from the stems versus leaves of this plant. In the current study, we prepared EAF by reflux extraction and sequential extraction from the stems (SEAF) and leaves (LEAF) of PCP and tested their hepatoprotective efficacies. The extract rates and flavonoid contents of LEAF were higher than those of SEAF. EAFs (>50 μg·mL ) prevented lipid accumulation in cells and protected against lipotoxicity injury when the concentration exceeded 25 μg·mL . More than 95% free radicals released by 2,2-diphenyl-1-picrylhydrazyl (DPPH) were eliminated by 25 μg·mL SEAF and 50 μg·mL LEAF, respectively. Further, EAFs (25 μg·mL ) also showed protective antioxidant effects, with the activity of LEAF being significantly higher than that of SEAF. EAFs (10 mg·mL ) also showed similar unspecific bacteriostatic activity. In comparison with SEAF, LEAF contained more flavonoids and had a higher anti-oxidation capability and for these reasons we suggest it should be better for clinical use.

关键词： antibacterial     anti-oxidation     lipid accumulation     lipotoxicity     Penthorum chinense Pursh    

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Evaluation of precipitation behavior of zirconium molybdate hydrate

Liang ZHANG, Masayuki TAKEUCHI, Tsutomu KOIZUMI, Izumi HIRASAWA

《化学科学与工程前沿（英文）》 2013年 第7卷 第1期   页码 65-71 doi: 10.1007/s11705-013-1314-9

摘要： In the dissolution step of spent nuclear fuel, there is a world-concern problem that zirconium molybdate hydrate precipitates as a byproduct, and accumulates in some reprocessing equipments. In order to prevent this accumulation, we have developed a new method based on the controlled reaction crystallization of zirconium molybdate hydrate (ZMH) in the reprocessing solution, followed by solid liquid separation. In order to measure the particle size of ZMH, batch crystallization experiments were conducted by varying nitric acid concentration and operating temperature. In result, almost all particle sizes scatter around 1 μm on average, despite the higher concentration of nitric aid and operating temperature, and then small particles grow up as an aggregate sticking to the crystallizer. Moreover, polymorph and color changing were observed by varying the concentration of nitric acid and reaction time. These results suggest that crystal color and adhesiveness are closely related to the particle size of ZMH. And the control of nitric acid concentration and small particle growth would be the useful technique to prevent the ZMH sticking.

关键词： spent nuclear fuel     zirconium molybdate hydrate     cleaning method     accumulation    

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标题 作者 时间 类型 操作

Optimization of methyl orange removal from aqueous solution by response surface methodology using spenttea leaves as adsorbent

Liangzhi LI,Xiaolin LI,Ci YAN,Weiqiang GUO,Tianyi YANG,Jiaolong FU,Jiaoyan TANG,Cuiying HU

期刊论文

Separation of epigallocatechin-3-gallate from crude tea polyphenols by using Cellulose diacetate graft

Hong ZHU, Peiyong QIN

期刊论文

Investigation of phosphate adsorption from an aqueous solution using spent fluid catalytic cracking catalyst

Zhen Li, Zhaofu Qiu, Ji Yang, Benteng Ma, Shuguang Lu, Chuanhui Qin

期刊论文

APPLICATION AND DEVELOPMENT OF ‘GREEN’ PREVENTIVE AND CONTROL TECHNOLOGIES IN GUIZHOU TEA PLANTATIONS

期刊论文

INTERCROPPING TEA PLANTATIONS WITH SOYBEAN AND RAPESEED ENHANCES NITROGEN FIXATION THROUGH SHIFTS IN

期刊论文

APPLICATION AND DEVELOPMENT OF ‘GREEN’ PREVENTIVE AND CONTROL TECHNOLOGIES IN GUIZHOU TEA PLANTATIONS

期刊论文

GASEOUS REACTIVE NITROGEN LOSSES FROM ORCHARDS, VEGETABLES AND TEA PLANTATIONS

期刊论文

Preparing graphene from anode graphite of spent lithium-ion batteries

Wenxuan Zhang, Zhanpeng Liu, Jing Xia, Feng Li, Wenzhi He, Guangming Li, Juwen Huang

期刊论文

TRANSCRIPTOME ANALYSIS REVEALS METABOLITE VARIATION AND FLAVONOID REGULATORY NETWORKS IN FRESH SHOOTS OF TEA

期刊论文

TRANSCRIPTOME ANALYSIS REVEALS METABOLITE VARIATION AND FLAVONOID REGULATORY NETWORKS IN FRESH SHOOTS OF TEA

Chen-Kai JIANG, De-Jiang NI, Ming-Zhe YAO, Jian-Qiang MA, Liang CHEN

期刊论文

Highly selective metal recovery from spent lithium-ion batteries through stoichiometric hydrogen ion

Weiguang Lv, Xiaohong Zheng, Li Li, Hongbin Cao, Yi Zhang, Renjie Chen, Hancheng Ou, Fei Kang, Zhi Sun

期刊论文

Bioleaching of spent Ni-Cd batteries and phylogenetic analysis of an acidophilic strain in acidified

ZHAO Ling, WANG Liang, YANG Dong, ZHU Nanwen

期刊论文

Alcohol and tea consumption in relation to the risk of nasopharyngeal carcinoma in Guangdong, China

Hong-Lian RUAN, Feng-Hua XU, Wen-Sheng LIU, Qi-Sheng FENG, Li-Zhen CHEN, Yi-Xin ZENG, Wei-Hua JIA,

期刊论文

A comparison of the biological activities of ethyl acetate fractions from the stems and leaves of

Zhaolei WANG, Kai JIANG, Qinchao DING, Shujun LIU, Xiaobing DOU, Bin DING

期刊论文

Evaluation of precipitation behavior of zirconium molybdate hydrate

Liang ZHANG, Masayuki TAKEUCHI, Tsutomu KOIZUMI, Izumi HIRASAWA

期刊论文